Gravimetric determination of phosphorus in fertilizer samples
In Gravimetric Analysis, the product with known composition is resulted from the conversion of the analyte to a soluble precipitate that can be easily filtered and is free from impurities by subjecting it to heat.
Filterability improves as the crystal size increases. As this happens, the size of this layer increases and the strong repulsive forces, which make the original colloidal state, are reestablished. Digestion is necessary to let reprecipitation. This product of known composition will then be weighed and the percentage of the analyte in the sample can be determined. The crucible with the fertilizer was weigh. The filter paper that was preweighed was kept in the dessicator until further use to keep the moisture from adhering to the filter paper. White precipitate was formed.Accessed 04 January Words:Paragraphs: 37, Pages: 8 Publication date: January 04, Sorry, but copying text is forbidden on this website! However, the usual types of fertilizers with phosphates contain a minimum of An Ethanol Molecule Then, the precipitate was then put into an oven.
The cooling of the crucible is crucial to avoid errors caused by air currents. In nucleation, particles join together to form a large mass, usually a result of supersaturation in solutions. After the initial weigh in, the whole heating-cooling-weighing is repeated until a constant weight was observed. The solution was filter using the pre-weighed filter paper. It was then transferred to the desiccator for 15mins. Preparation and Constant Weighing of Crucibles Crucible with cover was thoroughly wash and clean. This product of known composition will then be weighed and the percentage of the analyte in the sample can be determined. Prepare a vacuum filtration apparatus using a buchner funnel. It should be noted that NH3 is added slowly with continuous stirring to the solution to ensure the growth of the precipitate, resulting to a precipitate that is easier to filter and be freed of impurities.Even though Gravimetry is considered as one of the efficient and less expensive ways of finding a fertiliser constituent. The filter paper that was preweighed was kept in the dessicator until farther usage to maintain the wet from adhering to the filter paper.
Discussion This experiment aims to find the per centum of P and P2O5 in fertiliser sample utilizing Gravimetry. Also, because of this rejection in data, aside from the fact that Data Set 2 has lower number of population, Data Set 2 parameters for Measure of Precision are closer to each other, with the dried samples having greater values than that of the wet sample.
Gravimetric determination of phosphorus in fertilizer samples
See Equation 1. One of these mistakes is the fast add-on of the precipitating agent and low impact of agitation that leads to the production of larger sum of little atoms that may go through through the filter paper therefore holding lesser sum of precipitate. The dried sample from the old experiment from which wet was determined. There may be a small amount of insoluble residue. A constant weight will be obtain if the next weight is within the range of 0. Results were tabulated. In the experiment, stirring was done while adding NH3. In Gravimetric Analysis. The crucible was transfer to a desiccator and was allow to cool for 15minutes.This implies that Q should be relatively higher than S. Fundamentals of Analytic Chemistry, 8th ed. A white precipitate, magnesium ammonium phosphate hexahydrate, was formed.
The filter paper used was weighed to easy find the weight of the precipitate.